MS Report from Instrument: LCMS-03 File ..\\2018\\20180802\\20180802\\CPK2018-802-18566.D Tgt Mass (CHM): Injection Date : 2 Aug 18 2:45 pm +0800 Seq. Line : 66 Sample Name : CPK2018-802-18566 Location : P2-E-03 Acq. Operator : SYSTEM Inj : 1 Spec. Reported : MS Integration Inj Volume : 2 ul Acq. Method : D:\\LCMS03\\Data\\2018\\20180802\\20180802\\1-POS-3MIN.M Analysis Method : D:\\LCMS03\\Data\\2018\\20180802\\20180802\\1-POS-3MIN.M Catalog No : HY-16962 Batch#18566 Method Info : Mobile Phase: A: water(0.01%TFA) B:ACN(0.01%TFA) Gradient: 5% to 95%B within 1.3 min Flow Rate :1.8ml/min Column :SunFire C18, 4.6*50mm,3.5um A-RP-186 Oven Temperature : 45C DAD1 A, Sig=214,4 Ref=off100050000.5061.3151.2741.42511..457080mAU00.5 DAD1 B, Sig=2,4 Ref=offmAU50011.3151.522.5min1.2741.4251.4771.5001.1531.6061.922250000.5 ELS1 A, ELSD SignalmV201000.51 MSD1 TIC, MS File ES-API, Pos, Scan, Frag: 701000000500000012.0311.51.40422.5min1.51.34122.5min1.4711.88400.511.5 Ion 337.4, MSD1 337.4,Target Mass 336.4 +H Positive, EIC=337.1:338.1750000500000250000000.51 Integration Results for DAD1 A, Sig=214,4 Ref=off1.33822.5min1.522.5min RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 0.51 0.02 3.26 2.71 0.17 102 1.27 0.02 30.81 30.95 1.61 337 1.31 0.02 1853.21 11.95 96. 337 1.42 0.02 12.21 8.02 0. 337 1.48 0.01 0.76 1.13 0.04 451 1.50 0.02 17.46 12.66 0.91 3 Integration Results for DAD1 B, Sig=2,4 Ref=off RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 1.15 0.02 0.59 0.48 0.07 102 1.27 0.02 20.91 20.81 2.32 337 1.31 0.02 860.09 755.25 95. 337 1.42 0.02 6.14 3.68 0.68 337 1.48 0.01 0.45 0. 0.05 451 1.50 0.02 8.04 5.31 0. 3 1.61 0.02 1.39 0.83 0.16 102 1.92 0.02 0.88 0.61 0.10 233LCMS-03 8/2/2018 3:12:05 PM SYSTEMPage1 of4MS Report from Instrument: LCMS-03 2.03 0.02 0.82 0.70 0.09 233 Integration Results for ELS1 A, ELSD Signal RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 1.40 0.06 91. 24. 100.00 337 Integration Results for MSD1 TIC, MS File RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 1.34 0.06 56700.50 1433420.50 95.96 337 1.47 0.17 150539.53 14871.20 2.55 451 1.88 0.08 88238. 26332.62 1.49 233LCMS-03 8/2/2018 3:12:05 PM SYSTEMPage2 of4MS Report from Instrument: LCMS-03Ret. Time: 1.34 <<<< POSITIVE SPECTRA >>>> ES-API Positive20000017500015000012500075000250000100200300400500600700800900m/z102.250000169.1701.5695.3355.1452.2451.2233.1130.1337.1100000338.1337.1 ES-API Positive102.21600014000120001000080006000279.1157.1328.1234.1103.2199.1400020000100200300400500600700800900m/zRet. Time: 1.47730.3370.4Ret. Time: 1.88 ES-API Positive20000175001500012500100007500130.1261.1588.1157.1217.1337.0103.2370.4609.0500025000100200300400500600700m/z234.1102.2233.1105.1421.2471.14.1LCMS-03 8/2/2018 3:12:05 PM SYSTEMPage3 of4923.3MS Report from Instrument: LCMS-03 *** End of Report ***LCMS-03 8/2/2018 3:12:05 PM SYSTEMPage4 of4
