RG2833_LCMS_09491_MedChemExpress

Data File D:\\AGLIENT 1260\\DATA\\20150526\\20150525 2015-05-26 13-55-34\\CPK2015-526-09491.DSample Name: CPK2015-526-09491=====================================================================Acq. Operator : Li Shan(LCMS-02) Seq. Line : 30Acq. Instrument : HY-LCMS-02 Location : P1-B-02Injection Date : 5/26/2015 4:00:48 PM Inj : 1 Inj Volume : 3.000 µlAcq. Method : D:\\AGLIENT 1260\\DATA\\20150526\\20150525 2015-05-26 13-55-34\\100-1000MS+3MIN- 1.5_(0.02%FA).MLast changed : 5/26/2015 1:55:35 PM by Li Shan(LCMS-02)Analysis Method : D:\\AGLIENT 1260\\METHOD\\HM-375_6-H01RS10(RP-HPLC.).MLast changed : 5/27/2015 4:43:24 PM by Li Shan(LCMS-02) (modified after loading)Method Info : Negtive,MS:100-1000,Column ID:A-RP108 40℃ Catalo No : HY-125 Batch#09491 A-RP-132 Additional Info : Peak(s) manually integrated DAD1 C, Sig=2,4 Ref=off (D:\\AGLIENT...0\\DATA\\20150526\\20150525 2015-05-26 13-55-34\\CPK2015-526-09491.D) 1.788mAU1000800600400 2.035 1.599 1.697 2.13720000.511.522.53min ===================================================================== Area Percent Report ===================================================================== Sorted By : SignalMultiplier : 1.0000Dilution : 1.0000Do not use Multiplier & Dilution Factor with ISTDs Signal 1: DAD1 C, Sig=2,4 Ref=off Peak RetTime Type Width Area Height Area # [min] [min] [mAU*s] [mAU] %----|-------|----|-------|----------|----------|--------| 1 1.599 MM R 0.0408 5.11204 2.08715 0.1518 2 1.697 MM R 0.0410 5.04202e-1 2.05146e-1 0.0150 3 1.788 MM R 0.0463 3349.42188 1206.34839 99.4280 4 2.035 MM R 0.0501 11.06848 3.68348 0.3286 5 2.137 MM R 0.0448 2.58325 9.60926e-1 0.0767 Totals : 3368.685 1213.28509 ===================================================================== *** End of Report ***HY-LCMS-02 5/27/2015 4:43:25 PM Li Shan(LCMS-02)Page 1 of 1

Data File D:\\AGLIENT 1260\\DATA\\20150526\\20150525 2015-05-26 13-55-34\\CPK2015-526-09491.DSample Name: CPK2015-526-09491==========================================================Acq. Operator : Li Shan(LCMS-02) Seq. Line : 30Acq. Instrument : HY-LCMS-02 Location : P1-B-02Injection Date : 5/26/2015 4:00:48 PM Inj : 1 Inj Volume : 3.000 µlAcq. Method : D:\\AGLIENT 1260\\DATA\\20150526\\20150525 2015-05-26 13-55-34\\100-1000MS+3MIN- 1.5_(0.02%FA).MLast changed : 5/26/2015 1:55:35 PM by Li Shan(LCMS-02)Analysis Method : D:\\AGLIENT 1260\\METHOD\\HM-375_6-H01RS10(RP-HPLC.).MLast changed : 5/27/2015 4:44:28 PM by Li Shan(LCMS-02) (modified after loading)Method Info : Negtive,MS:100-1000,Column ID:A-RP108 40℃ Catalo No : HY-125 Batch#09491 A-RP-132 Additional Info : Peak(s) manually integrated MSD1 TIC, MS File (D:\\AGLIENT 1260\\DATA\\20150526\\20150525 2015-05-26 13-55-34\\CPK2015-526-09491.D) ES-API, Pos, Sc 1.783100000080000060000040000020000000.511.522.53min HY-LCMS-02 5/27/2015 4:44:30 PM Li Shan(LCMS-02)Page 1 of 2

Data File D:\\AGLIENT 1260\\DATA\\20150526\\20150525 2015-05-26 13-55-34\\CPK2015-526-09491.DSample Name: CPK2015-526-09491MS Signal: MSD1 TIC, MS File, ES-API, Pos, Scan, Frag: 50 Spectra averaged over upper half of peaks. Noise Cutoff: 1000 counts. Reportable Ion Abundance: > 10%. Retention Mol. WeightTime (MS) MS Area or Ion 1.783 5209706 341.20 I 340.20 I*MSD1 SPC, time=1.762:1.817 of D:\\AGLIENT 1260\\DATA\\20150526\\20150525 2015-05-26 13-55-34\\CPK2015-526-09491.D ES-API100806040200100200300400500600700800m/z 341.2 340.2Max: 596848 *** End of Report ***HY-LCMS-02 5/27/2015 4:44:30 PM Li Shan(LCMS-02)Page 2 of 2